In Powder Metals (PM) applications such as 3D printing, the flow and packing behavior of PM is influenced by particle size and shape distributions. These properties can be measured in a statistically meaningful way using computer controlled scanning electron microscopy (CCSEM). In livetime, the SEM program detects a particle, defines its perimeter, calculates its size and shape properties, and saves the particle image. The shape properties quantified are elongation (aspect ratio), roundness, and form factor, as defined in ASTM F1877 Standard Practice for Characterization of Particles. All particles in a microscope field are processed, and additional fields are processed until the stopping criterion is met. Figure 1 below shows CCSEM results of a powder sample. The shape distributions are shown for the smallest 25%, the medium 50%, and the largest 25%.
Review of the acquired images supplies a “ground truth” function to provide reality to the numeric descriptors. Figure 5 demonstrates that the Roundness value in this set of samples is primarily related to small satellites on the particle, with the size and number of fused satellites increasing with decreasing roundness. The roundness values of powder of different composition, manufactured by other techniques, or reused through multiple build cycles, may display other surface features.
These distributions can be used to compare samples, or define changes in shape with particle size. Table 1 shows the definitions of Large, Medium and Small, as well as the average values for the three shape measures. Table 1 and Figure 6 show that the smaller particles deviate from a perfect circle more than larger particles.
Although SEM field images can be used to qualitatively assess the size and shape distribution in a general way, the CCSEM size/shape analysis can quantify shape on a particle-by-particle basis, resulting in a complete shape distribution and a deeper understanding of the powder, including insight into the origin in any differences in shape. This information may be critical in understanding the flow of powder in the printer and build box, the powder-bed density, and the quality of the final product. This can be applied as a tool in
assessing or qualifying virgin powder, or changes in powder that has undergone multiple build cycles.
Compositional information can also be performed with the particle-by-particle analysis using EDS. This will allow investigation of changes in powder metal composition, or the presence of extraneous particulate. The experts at RJ Lee Group can work with your team to answer questions and find solutions for your powder metal manufacturing facility. Call us today at 1.800.860.1775, ext. 4, then 2, then 1, or click on the button below to learn more.