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RJ Lee Group, Inc
September 9, 2010 | Contact Us
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With expertise across multiple disciplines, RJLG has the resources to develop innovative methodologies for implementing specialized research studies and for solving unique problems. Our experienced staff is capable of developing a solution to meet your unique materials characterization requirements.
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Method Development for Medical Device Testing
The FDA approval requirements are continually evolving as innovation in the medical industry produces new devices, requiring new testing. Through various analytical methods and instrumentation, RJ Lee Group (RJLG) has generated new testing programs to evaluate those devices. Working hand-in-hand with our clients has allowed us to design, verify and implement protocols to effectively measure performance under rigorous testing. Through method development and ensuing consultation, we have delivered various product and process solutions for meeting FDA approval.
Monthly Environmental Monitoring at a Hospital Medical Center Pharmacy Compounding Area
RJ Lee Group (RJLG) performs environmental monitoring in the pharmacy compounding area at hospitals to assess compliance with the United States Pharmacopeia (USP) Standard 797 section on Environmental Quality and Control, subsection Environmental Monitoring. The collection of active air samples and surface samples for viable microorganisms is conducted in each controlled air environment every month. The controlled air environments include laminar airflow workbenches (LAFWs), biological safety cabinets (BSCs), buffer areas, and ante areas. An Andersen N-6 Single Stage Impactor and calibrated sampling pump are utilized to collect air samples and surface samples are collected using replicate organism detection and counting (RODAC) contact plates. Particle count readings are also obtained in each controlled air environment for comparison with the International Standards Organization (ISO) classifications for clean rooms. A report containing the test results and recommendations for correcting deficiencies is issued each month.
Patent Infringement Claim
An organic product producer and patent holder claimed that a competitor was utilizing protected technology to produce their goods. RJ Lee Group's (RJLG) team of experts designed extensive sampling and testing programs to determine the scientific validity of the claim. Over the course of five months our sampling team collected over 1000 samples at nearly 200 locations. The samples were analyzed using gas chromatography (GC), scanning electron microscopy (SEM) and optical microscopy. RJLG's scientists provided expert testimony.
Petrographic Analysis of WTC Concrete
The World Trade Center destruction on September 11, 2001, physically destroyed significant portions of the interior and exterior of the building located at 130 Liberty Street, New York, NY. The collapse of the south tower crushed into the North side of the 130 Liberty building creating a gash from the 5th to 23rd floors and collapsed the plaza area in front, exposing the basement area. Over 1,500 additional windows were broken. A 20,000-gallon diesel fuel tank in the northwest corner of the upper basement area (Level A) ruptured during the collapse of the south tower. Fuel spilled onto Level A and then through the collapsed floor, settling in the lower basement area (Level B). Some of the fuel ignited in Level B and burned along with other debris and materials damaging steel beams and concrete elements. Water from various sources was also introduced into Level B. Thus, a fuel and water mixture soaked into and saturated the concrete foundation in Level B for approximately 2 and a half months.

Petrographic analyses of the foundation concrete (walls and slabs) examined the extent of deleterious phases and the extent of cracking throughout the structural members. The analyses showed expansive, damaging chemical reactions known as alkali silica reaction (ASR) and delayed ettringite formation (DEF) to be ongoing. These water driven reactions caused cracking, expansion and deterioration of the concrete. Large cracks, observed by optical microscopy, were primarily associated with ASR reactive aggregate. The most deteriorated sections of the foundation were in areas of maximum debris impact and fire damage. Unfilled cracks, observed by scanning electron microscopy (SEM), are indicative of cracking induced by the collapse impact and/or the ongoing chemical reactions. An investigation of physical properties of the foundation concrete confirmed the conclusions from petrography. Results indicated that the impact of debris, the exposure to fire and the deleterious reactions have severely reduced the engineering properties of the concrete. Very high porosities, ionic diffusion coefficients and moisture transport values were measured for samples extracted from the fire damage and the impact damaged areas.

Petrographic Examination of Parking Garages and Other Large Concrete Structures

As deterioration of concrete occurs on large concrete structures, repair and future preventative action depends on a thorough understanding of the cause of the failure. RJ Lee Group (RJLG) has leveraged extensive petrography experience to analyze concrete failures and identify their causes. This skillset enabled RJLG to assist a parking garage manager protect the facility.  Visual observations, optical microscopy, and scanning electron microscopy with energy dispersive X-ray microanalyses have all contributed to the forensic investigation. Through source determination of the failure, RJLG provided the facility manager with the information necessary to effectively repair or replace the damaged cement.

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